Investigation of the Hydrophobic Properties Stability of Textured Polymer Coatings Deposited on the Track-Etched Membrane Surface

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Тек жазылушылар үшін

Аннотация

The stability of the hydrophobic properties of coatings with a morphologically developed (textured) surface prepared from polytetrafluoroethylene and ultra-high molecular weight polyethylene during storage, as well as during prolonged contact with water and aqueous solutions of sodium chloride with concentrations from 5 to 15 g/L has been studied. These coatings were deposited on the surface of a poly(ethylene terephthalate) track-etched membrane by electron-beam dispersion of the pristine polymers in vacuum. It is found that coatings from polytetrafluoroethylene under the influence of real environmental conditions tend to age and gradually lose their hydrophobic properties. The water contact angle of the coatings decreases by an average of 30° during storage samples of composite membranes for 5 years. This is 23% of the pristine value. The decrease in the contact angle of coatings of this type is due to the transition from a heterogeneous wetting mode to a homogeneous one, the reason for which is the formation of an adsorption layer of water on their surface. In contrast, the water contact angle for coatings from ultra-high molecular weight polyethylene practically does not change during storage of membrane samples. A study of the polymer coatings stability during prolonged contact of composite membranes with water and aqueous solutions of sodium chloride showed that if coatings from ultra-high molecular weight polyethylene are stable in both water and aqueous solutions of sodium chloride, then coatings from polytetrafluoroethylene are more stable to the action of aqueous salt solutions than water.

Толық мәтін

Рұқсат жабық

Авторлар туралы

L. Kravets

Flerov Laboratory of Nuclear Reactions of the Joint Institute for Nuclear Research

Хат алмасуға жауапты Автор.
Email: kravets@jinr.ru
Ресей, Dubna, 20, Joliot-Curie St., 141980

M. Yarmolenko

Francisk Skorina Gomel State University

Email: kravets@jinr.ru
Белоруссия, Gomel, 104, Sovetskaya St., 246019

A. Rogachev

Francisk Skorina Gomel State University

Email: kravets@jinr.ru
Белоруссия, Gomel, 104, Sovetskaya St., 246019

R. Gainutdinov

Crystalography and Photonics Federal Research Centre of the Russian Academy of Sciences

Email: kravets@jinr.ru
Ресей, Moscow, 59, Leninsky Ave., 119333

M. Kuvaytseva

Flerov Laboratory of Nuclear Reactions of the Joint Institute for Nuclear Research

Email: kravets@jinr.ru
Ресей, Dubna, 20, Joliot-Curie St., 141980

V. Altynov

Flerov Laboratory of Nuclear Reactions of the Joint Institute for Nuclear Research

Email: kravets@jinr.ru
Ресей, Dubna, 20, Joliot-Curie St., 141980

N. Lizunov

Flerov Laboratory of Nuclear Reactions of the Joint Institute for Nuclear Research

Email: kravets@jinr.ru
Ресей, Dubna, 20, Joliot-Curie St., 141980

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2. Fig. 1. SEM images of the surface layer of the original PET TM with a pore diameter of 250 nm (a), 300 (b) and 500 nm (c) UHMWPE-coated membranes; 300 (d) and 500 nm (e) PTFE-coated membranes; and the reverse side of the modified membrane (f).

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3. Fig. 2. Three-dimensional AFM-derived surface images of PET TM with a pore diameter of 250 nm after 300 (a) and 500 nm (b) UHMWPE coating, after 300 (c) and 500 nm (d) PTFE coating; scanned directly after fabrication of membrane samples.

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4. Fig. 3. Condensate flux variation in time during membrane distillation of initial PET and PP track membranes (a) and composite membranes with 300 (1) and 500 nm (2) thick PTFE coating, 300 (3) and 500 nm (4) thick UHMWPE coating deposited by ELD method (b)

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5. Fig. 4. Variation of water wetting angle (a), LEPW value (b) and surface roughness (c) of UHMWPE and PTFE coatings as a function of their thickness during storage of composite membranes for 5 years.

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6. Fig. 5. Three-dimensional AFM-derived surface images of PET TM with 250 nm pore diameter after 300 (a) and 500 nm (b) UHMWPE coating, after 300 (c) and 500 nm (d) PTFE coating; scans were taken after membrane samples had been stored for 5 years.

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7. Fig. 6. RFES spectra of C1s atoms of 500 nm thick UHMWPE (a) and PTFE (b) coatings deposited by electron-beam dispersion; measured after storage of composite membranes for 5 years.

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